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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
19 April to 21 May, 2002
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
other: GLP study according to internally accepted guidelines.

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2002
Report date:
2002

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
capillary method

Test material

Constituent 1
Chemical structure
Reference substance name:
4-(Cyclopropylcarbonyl)-α,α-dimethyl-ethyl ester benzeneacetic acid
EC Number:
605-546-9
Cas Number:
169280-10-8
Molecular formula:
C16 H20 O3
IUPAC Name:
4-(Cyclopropylcarbonyl)-α,α-dimethyl-ethyl ester benzeneacetic acid
Details on test material:
Batch W 0147
Purity 98%
Stability: stable up to 500 °C, incompatible with bases
Solubility in water: < 1g/l

Results and discussion

Melting / freezing point
Melting / freezing pt.:
>= 56.1 - <= 58.3 °C

Applicant's summary and conclusion

Conclusions:
The melting range was determined as 56.1 - 58.3 °C, both values being the mean of two independent measurements.