Registration Dossier

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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2021
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2021

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
(4S)-1-methyl-4-(6-methylhepta-1,5-dien-2-yl)cyclohexene
EC Number:
610-461-5
Cas Number:
495-61-4
Molecular formula:
C15H24
IUPAC Name:
(4S)-1-methyl-4-(6-methylhepta-1,5-dien-2-yl)cyclohexene
Test material form:
liquid

Results and discussion

Melting / freezing point
Key result
Decomposition:
no
Sublimation:
no
Remarks on result:
other: No melting temperature was found between -120 °C and 40 °C

Any other information on results incl. tables

No melting temperature was found between -120 °C and 40 °C, even by addition of aluminum oxide powder as crystallization aid and annealing at -110 °C and -90 °C (determination Test 2).


Below -100 °C a glass transition was visible with an approximate value of -115 °C. Further analysis was not possible because the start of the glass transition lay outside of the instrument measuring range.


The estimated accuracy is ± 1 °C.

Applicant's summary and conclusion

Conclusions:
No melting temperature was found between -120 °C and 40 °C, even by addition of aluminum oxide powder as crystallization aid and annealing at -110 °C and -90 °C.