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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Physical & Chemical properties

Boiling point

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Administrative data

Link to relevant study record(s)

Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Justification for type of information:
Experimental test result performed using standard OECD test guidelines
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling point/boiling range)
GLP compliance:
no
Type of method:
method according to Siwoloboff
Key result
Boiling pt.:
> 250 °C
Atm. press.:
96 990 Pa
Remarks on result:
other: Other details not known

TEST DESCRIPTION AND RESULT

Method Details

Observations 

Remarks if, any

Guideline

OECD 103

-

 

Method

Method according to Siwoloboff

-

Principle of Boiling point test

The boiling point of a liquid is the temperature at which that liquid is converted to a gaseous state. It can be defined as the temperature at which the vapour pressure of the liquid becomes equal to the pressure at the surface of the liquid.

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Volume of chemical used

ml/ g

1 ml

Nature of the Bath taken

·    Oil bath

·    Water bath

Oil Bath

 

If oil bath is used, the type of oil

·    Liquid paraffin

·    Silicone oil

Silicone oil

Atmospheric pressure

hPa

969.9 hPa

Decomposition

Decomposition temperature (°C), if applicable

·                    Yes

·                    No

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Boiling point (°C) (RESULT)

°C

           >250

Conclusions:
The boiling point determination of test chemical was done following OECD Guideline 103 and according to the method of Siwoloboff. The mean boiling point was determined to be > 250°C at 96990 Pa.
Executive summary:

The boiling point of test chemical was determined. The study was performed in accordance with the OECD Guideline 103 (Boiling Point). The method followed was according to Siwoloboff. The mean boiling point was determined to be > 250°C  at 96990 Pa.

Description of key information

On the basis of available data from study report, the boiling point of test chemical was determined. The study was performed in accordance with the OECD Guideline 103 (Boiling Point). The method followed was according to Siwoloboff. The mean boiling point was determined to be > 250°C at 96990 Pa.

Key value for chemical safety assessment

Boiling point at 101 325 Pa:
250 °C

Additional information

On the basis of available data from study report, the boiling point of test chemical was determined. The study was performed in accordance with the OECD Guideline 103 (Boiling Point). The method followed was according to Siwoloboff. The mean boiling point was determined to be > 250°C at 96990 Pa.

In a supporting study fromhandbooks,the boiling point of test chemical was determined to be 246.0°C at 101325 Pa (760 mmHg).

Additional study from authoritative database indicates the boiling point of test chemical as 226.69°C estimated by adapted Stein and Brown method.